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US7569575B2 – Synthesis of locked nucleic acid derivatives. – After 4 h the reaction was completed and most of the DMF was remove in vacuo. The resulting slurry 81 was coevaporated twice from anh. pyridine (225 mL) and suspended in anh. pyridine (10 mL). 4,4-dimethoxytritylchloride (1.48 g, 4.37 mmol) was added and the reaction mixture was stirred for 16 h at rt.
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